2,4-Difluoroaniline
C6H5F₂N
CAS No.: 367-25-9


Application

Tert-butyl nitrite (2.58 mmol) was gradually added to a solution of 2,4-difluoroaniline (2.15 mmol) in anhydrous acetonitrile (8 ml) that had been allowed to cool to 0°C in an ice bath. into the agitated mixture, followed by the dropwise addition of azidotrimethylsilane (2.58 mmol) to the reaction mixture. For two hours, the resultant solution was swirled at room temperature. The reaction mixture was immediately concentrated under vacuum following the reaction. To get the desired product molecule, the resultant residue was separated and purified using silica gel chromatography (hexane).
Physical Properties
|
MF |
C6H5F₂N |
|
Boiling point |
168.4±20.0 °C at 760 mmHg |
|
Density |
1.3±0.1 g/cm³ (Predicted) |
|
Appearance |
Coloress clear liquid |
|
Molecular mass |
129.11 |
|
Assay |
≥99% |
|
Package |
50kgs or according customer requirement |
|
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|
Chemical Safety

GHS Hazard Statements
|
H302 (100%) |
Harmful if swallowed [warning Acute toxicity, oral] |
|
H312 (100%) |
Harmful in contact with skin [warning Acute toxicity, dermal] |
|
H315 (89.36%) |
Causes skin irritation [warning Skin corrosion/irritation] |
|
H318 (87.23%) |
Causes serious eye damage [Danger Serious eye damage/eye irritation] |
|
H332 (91.49%) |
Harmful if inhaled [warning Acute toxicity, inhalation] |
|
H335 (100%) |
May cause respiratory irritation [warning Specific target organ toxicity, single exposure; Respiratory tract irritation] |




Packing, Storage, Handling and Transportation
Hexafluorobenzene should be sealed in dry place at room temperature.

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