2,6-Difluorobenzyl Alcohol ≥99.5%

C₇H₆F₂O CAS NO.19064-18-7

product-713-788

Application

Lithium aluminum hydride was reduced to create 2,6-Difluorobenzylamine. The target compound can be verified using infrared, nuclear magnetic, and other analytical techniques, and the reaction is simple to conduct and has mild conditions.‌

Next, 2,6-difluorobenzyl alcohol can be prepared by reacting a Grignard reagent with 2,6-difluorobenzylamine. The specific steps are as follows:

1.In the presence of organic or inorganic solvents, add compound 2,6-difluorotoluene and hydrobromic acid, add hydrogen peroxide dropwise under light conditions, and react for 6 to 24 hours.

2.The reaction solution was washed with saturated sodium sulfite solution and water respectively, dried over anhydrous sodium sulfate, and then the solvent was evaporated under reduced pressure.

3.Compound 2,6-difluorobenzene bromide was obtained by silica gel column chromatography‌.

Physical Properties

Boiling point	188.6±25.0 ℃ at 760 mmHg
Density	1.3 g/mL at 25 °C(lit.)
Molecular mass	144.12
Assay	≥99.5%
Flash point	192℉
Water solubility	Not miscible or difficult to mix in water
Refractive index	N20/D 1.495(lit.)
Package	50kgs or according customer requirement
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